1-苯基-4-戊烯-1-炔合成路线 （共 44 条）
反应条件
Ni(P(OC3H7-i)3)4 in tetrahydrofuran
6 h; Heating;
参考文献
Leadbeater
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7539 - 7541
反应条件
[Pd{bis[2-(diphenylphosphino)phenyl] ether}Cl2] in tetrahydrofuran; N,N-dimethyl-formamide
T=70°C; 10 h;
参考文献
Qian, Mingxing; Negishi, Ei-Ichi
Synlett, 2005 , # 11 art. no. Y00105ST, p. 1789 - 1793
反应条件
bis(acetylacetonate)nickel(II); diisobutylaluminium hydride; triethyl phosphite in tetrahydrofuran; toluene
1 h; Heating;
参考文献
Cui, Dong-Mei; Hashimoto, Naoko; Ikeda, Shin-ichi; Sato, Yoshiro
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5752 - 5756
反应条件
bis(acetylacetonate)nickel(II); diisobutylaluminium hydride; triethyl phosphite in tetrahydrofuran; toluene
1 h; Heating;
参考文献
Cui, Dong-Mei; Hashimoto, Naoko; Ikeda, Shin-ichi; Sato, Yoshiro
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5752 - 5756
反应条件
in tetrahydrofuran; toluene
T=-45 - 20°C;
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A. A.; Wang, Mingyi
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7526 - 7529
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; copper(l) chloride in dichloromethane; water
T=20°C; 21 h; Yield given. Yields of byproduct given;
参考文献
Grushin, Vladimir V.; Alper, Howard
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2188 - 2192
反应条件
copper(l) iodide in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Kim, Won-Yeob; Jiao, Xianghua
Synthesis, 1998 , # 9 p. 1252 - 1254
反应条件
iron(II) sulfate; sodium nitrite in acetic acid
0.5 h; Ambient temperature;
参考文献
Boivin, Jean; Elkaim, Laurent; Ferro, Paul G.; Zard, Samir Z.
Tetrahedron Letters, 1991 , vol. 32, # 39 p. 5321 - 5324
参考文献
Bourguel; Piaux
Bulletin de la Societe Chimique de France, 1935 , vol. <5>2, p. 1966
Full Text Show Details
Grignard; Lapayre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1931 , vol. 192, p. 251
反应条件
bis(acetylacetonate)nickel(II); triphenylphosphine in tetrahydrofuran
-5 deg C, 15 min; 50 deg C, 4 h;
参考文献
Dzhemilev, U. M.; Ibragimov, A. G.; Saraev, R. A.; Minsker, D. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 835 - 836
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 4 p. 907 - 908
