(S)-(-)-1, 2, 4-丁三醇合成路线 (共 37 条)
反应条件
boric acid trimethyl ester; dimethylsulfide borane complex in tetrahydrofuran T=-5°C; 51 h;
参考文献
Shishido, Kozo; Sukegawa, Yuko; Fukumoto, Keiichiro; Kametani, Tetsuji
Heterocycles, 1986 , vol. 24, # 3 p. 641 - 645
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=65°C; 72 h;
参考文献
Boerjesson, Lena; Welch, Christopher J.
Tetrahedron, 1992 , vol. 48, # 30 p. 6325 - 6334
反应条件
sodium borohydride in methanol; toluene
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
tert.-butylhydroperoxide; potassium hydride in N,N-dimethyl-formamide
参考文献
Liu, Dong; Kozmin, Sergey A.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 24 p. 4757 - 4759
反应条件
E. coli DH5α; pWN6.186A in water T=33°C; ambient pressure;
参考文献
Niu, Wei; Molefe, Mapitso N.; Frost
Journal of the American Chemical Society, 2003 , vol. 125, # 43 p. 12998 - 12999
反应条件
LiAlH4 in tetrahydrofuran; dry-THF; water
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium hydroxide; PEP; adenosine 5'-triphosphoric acid; magnesium chloride in water T=27°C; 216 h; pH=7.5; Yield given. Yields of byproduct given;
参考文献
Crans, Debbie C.; Whitesides, George M.
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7019 - 7027
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=25°C; 3 h;
参考文献
Seki, Masahiko; Kondo, Kazuhiko
Synthesis, 1999 , # 5 p. 745 - 747