(S)-(-)-1, 2, 4-丁三醇合成路线 (共 37 条)
反应条件
(R,R)-N-lt;3,5-di-t-butyl-6-(11-(silica-O-SiMe2-linked)undecyloxy)gt;benzylidene-N'-(3-t-butyl-2,5-dihydroxy)benzylidene-1,2-cyclohexanediamine - (acetoxy)Co; water in tetrahydrofuran Ambient temperature; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Annis, D. Allen; Jacobsen, Eric N.
Journal of the American Chemical Society, 1999 , vol. 121, # 17 p. 4147 - 4154
参考文献
White, James D.; Kawasaki, Motoji
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5292 - 5300
反应条件
hydrogen; palladium on activated charcoal in methanol 5 h; Yield given. Yields of byproduct given;
参考文献
Cardillo, Giuliana; Orena, Mario; Romero, Marta; Sandri, Sergio
Tetrahedron, 1989 , vol. 45, # 5 p. 1501 - 1508
反应条件
boric acid trimethyl ester; dimethylsulfide borane complex in tetrahydrofuran Ambient temperature;
参考文献
Rodriguez, Evelyn B.; Scally, Gavin D.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 8 p. 1391 - 1405
反应条件
dimethylsulfide borane complex in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Lei, Ping-Sheng; Ogawa, Yuji; Kovac, Pavol
Journal of Carbohydrate Chemistry, 1996 , vol. 15, # 4 p. 485 - 500
反应条件
sodium tetrahydroborate
参考文献
Izquierdo, Isidoro; Plaza, Maria T.; Robles, Rafael; Rodriguez, Concepcion
Tetrahedron Asymmetry, 1996 , vol. 7, # 12 p. 3593 - 3604
反应条件
dimethylsulfide borane complex Moriwaki's procedure;
参考文献
Prasad, Kapa; Chen, Kau-Ming; Repic, Oljan; Hardtmann, Goetz E.
Tetrahedron: Asymmetry, 1990 , vol. 1, # 5 p. 307 - 310
参考文献
Kobayashi, Yoshihisa; Czechtizky, Werngard; Kishi, Yoshito
Organic Letters, 2003 , vol. 5, # 1 p. 93 - 96
参考文献
Edwards; Entwistle; Ley; Owen; Perry
Tetrahedron Asymmetry, 1994 , vol. 5, # 4 p. 553 - 556
反应条件
sodium hydroxide; sodium azide; pyruvate kinase; Phosphoenolpyruvate; glycerol kinase from C. mycoderma; potassium chloride; adenosine 5'-triphosphoric acid; 2-hydroxyethanethiol; magnesium chloride; alkaline phosphatase 1.) H2O, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Keith Chenault; Chafin, Laura F.; Liehr, Sebastian
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 4039 - 4045