反应条件
in tetrahydrofuran under N2 atm. ClHgMo(CO)3Cp and TlBF4 were added to soln. (NEt4)2(Fe5MoC(CO)17) in THF at -5°C and stirred for 2 h; Et2O was added and mixt. was cooled for 2 h to -30°C, ppt. was filtered, filtrate was evapd. to dryness, residue was extd. with CH2Cl2, pentane was added at -30°C; elem. anal.;
参考文献
Reina, Roser; Rodriguez, Laura; Rossell, Oriol; Seco, Miquel; Font-Bardia, Merce; Solans, Xavier
Organometallics, 2001 , vol. 20, # 8 p. 1575 - 1579
