2,3,4,6-四邻苄基-alpha-d-吡喃葡萄糖合成路线 (共 34 条)
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
反应条件
diethylamino-sulfur trifluoride in tetrahydrofuran 0.333333 h; Ambient temperatureaddition at -30 deg C;
参考文献
Tetrahedron Letters, , vol. 26, # 1 p. 5 - 8
反应条件
tin(II) trifluoromethanesulfonate; diethylamino-sulfur trifluoride; triethylamine in diethyl ether; dichloromethane T=-60 - 0°C; Condensation; substitution; 27.3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 12 p. 2893 - 2902
反应条件
1: 69 percent / tri-n-butylphosphine / CH2Cl2 / 0.5 h / 0 °C
2: siver(I) triflate / diethyl ether / 2 h / Ambient temperature
3: 85 percent / H2 / 10percent Pd/C / tetrahydrofuran / 12 h / 25 °C
View Scheme
参考文献
Stewart,A.O.; Williams,R.M.
Journal of the American Chemical Society, 1985 , vol. 107, p. 4289