1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide; water T=20°C; Heck reaction; 0.25 h; 2: 2-methoxy-6-bromo-naphthalene With 4'-hydroxyacetophenone oxime palladacycle catalyst in N,N-dimethyl acetamide; water T=120°C; Heck reaction; 9 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
Viviano, Monica; Glasnov, Toma N.; Reichart, Benedik; Tekautz, Guenter; Kappe, C. Oliver
Organic Process Research and Development, 2011 , vol. 15, # 4 p. 858 - 870
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide T=20°C; Heck reaction; 0.25 h; 2: 2-methoxy-6-bromo-naphthalene With Kaiser oxime-derived complex on resin base in N,N-dimethyl acetamide T=120°C; Heck reaction; 14 h; Further stages. Title compound not separated from byproducts.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide T=20°C; Heck reaction; 0.25 h; 2: 2-methoxy-6-bromo-naphthalene With Kaiser oxime-derived complex on resin base in N,N-dimethyl acetamide T=120°C; Heck reaction; 24 h; Further stages. Title compound not separated from byproducts.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
