sulfuric acid; palladium 10 on activated carbon; hydrogen in ethyl acetate
参考文献
Prabhakar; Reddy, C. Bakki; Reddy, Ch. Maheedhara; Nageshwar; Devi, A. Sivalakshmi; Babu, J. Moses; Vyas; Sarma; Reddy
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 121 - 125
1.1: potassium sec-butoxide / dimethyl sulfoxide / 1 h / 50 - 60 °C 1.2: pH 2 2.1: hydrogen; palladium 10 on activated carbon; sulfuric acid / ethyl acetate 3.1: sulfuric acid 4.1: hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Prabhakar; Reddy, C. Bakki; Reddy, Ch. Maheedhara; Nageshwar; Devi, A. Sivalakshmi; Babu, J. Moses; Vyas; Sarma; Reddy
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 121 - 125
1.1: acetic acid; bromine / 0.5 h / 30 - 35 °C 2.1: acetic acid; tin / 3 h / 100 - 120 °C 3.1: potassium carbonate / acetone; water / 4 h / 10 - 50 °C / |Cooling 4.1: magnesium; iodine / tetrahydrofuran / 5 h / |Reflux 4.2: 1.75 h / 10 - 90 °C 4.3: 1 h / 20 °C 5.1: sodium hydroxide / water / 4 h 6.1: hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Prabhakar; Reddy, C. Bakki; Reddy, Ch. Maheedhara; Nageshwar; Devi, A. Sivalakshmi; Babu, J. Moses; Vyas; Sarma; Reddy
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 121 - 125
1.1: acetic acid; tin / 3 h / 100 - 120 °C 2.1: potassium carbonate / acetone; water / 4 h / 10 - 50 °C / |Cooling 3.1: magnesium; iodine / tetrahydrofuran / 5 h / |Reflux 3.2: 1.75 h / 10 - 90 °C 3.3: 1 h / 20 °C 4.1: sodium hydroxide / water / 4 h 5.1: hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Prabhakar; Reddy, C. Bakki; Reddy, Ch. Maheedhara; Nageshwar; Devi, A. Sivalakshmi; Babu, J. Moses; Vyas; Sarma; Reddy
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 121 - 125
