water in tetrahydrofuran slow addn. of 10 mmol of the Grignard reagent to a stirred soln. of borane in THF (40 mmol); the mixt. was poured into ice-water and acidified with 10percent HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;;
参考文献
Kabalka, George W.; Sastry, Usha; Sastry, K.A.R.; Knapp, Furn F.; Srivastava, Prem C.
Journal of Organometallic Chemistry, 1983 , vol. 259, # 3 p. 269 - 274
