in tetrahydrofuran
addn. of a soln. of SnCl4 to a soln. of organic compound under cooling, heating for 12 h under reflux; addn. of HCl, reccrystn., elem. anal.;
参考文献
Schneider-Koglin, Claudia; Mathiasch, Bernd; Draeger, Martin
Journal of Organometallic Chemistry, 1994 , vol. 469, # 1 p. 25 - 32
1.1: tetrahydrofuran / 3 h / Heating
1.2: 63 percent / tetrahydrofuran / 20 °C
2.1: 99 percent / Et3N / CH2Cl2 / 20 °C
View Scheme
参考文献
Katritzky, Alan R.; Witek, Rachel M.; Rodriguez-Garcia, Valerie; Mohapatra, Prabhu P.; Rogers, James W.; Cusido, Janet; Abdel-Fattah, Ashraf A. A.; Steel, Peter J.
Journal of Organic Chemistry, 2005 , vol. 70, # 20 p. 7866 - 7881
