1: With AlCl3, aluminium chloride in chlorobenzene
T=90°C; 2 h;
2: With trichlorophosphate
1.16667 h; Reflux;
参考文献
Cinelli, Maris A.; Li, Huiying; Chreifi, Georges; Martasek, Pavel; Roman, Linda J.; Poulos, Thomas L.; Silverman, Richard B.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 4 p. 1513 - 1530
1: Behandeln des Reaktionsgemisches mit Kalium-hexacyanoferrat(III) und wss. Natronlauge.
2: phosphorus (V)-chloride; phosphoryl chloride / 140 °C
View Scheme
参考文献
Capps
Journal of the American Chemical Society, 1947 , vol. 69, p. 179