3-苯基-2H-氮丙啶-2-甲醛合成路线 （共 5 条）
反应条件
boron trifluoride diethyl etherate in diethyl ether T=-50 - 20°C; 0.333333 h;
参考文献
Brahma, Sulagna; Ray, Jayanta K.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 2 p. 311 - 317
反应条件
sodium azide in dimethyl sulfoxide
T=10 - 30°C; 0.333333 h;
参考文献
Brahma, Sulagna; Ray, Jayanta K.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6575 - 6578
反应条件
sodium azide in dimethyl sulfoxide
T=10 - 30°C; 0.333333 h;
参考文献
Brahma, Sulagna; Ray, Jayanta K.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6575 - 6578
反应条件
1: Br2 / CH2Cl2 / 0.33 h / 0 °C
2: NaN3 / dimethylsulfoxide / 24 h / 20 °C
3: aq. NaOH / dimethylsulfoxide / 92 h / 0 °C
4: 55 percent / MnO2 / CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Alajarin, Mateo; Orenes, Raul-Angel; Vidal, Angel; Pastor, Aurelia
Synthesis, 2003 , # 1 p. 49 - 52
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride
T=25°C;
参考文献
Padwa, Albert; Stengel, Thomas
Tetrahedron Letters, 2004 , vol. 45, # 31 p. 5991 - 5993
