1: CH2-indene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Metallation; 2 h;
2: dimethylmono-chlorosilane in tetrahydrofuran; hexane
T=20°C; silylation; 12 h; Further stages. Title compound not separated from byproducts.;
参考文献
Eppinger, Joerg; Spiegler, Michael; Hieringer, Wolfgang; Herrmann, Wolfgang A.; Anwander, Reiner
Journal of the American Chemical Society, 2000 , vol. 122, # 13 p. 3080 - 3096