6-乙酰氧基甲基苯并(a)芘合成路线 (共 4 条)
反应条件
in acetic acid
T=40°C; 0.5 h; Further byproducts given. Yields of byproduct given;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
in acetic acid
T=40°C; 1 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
1: 6-Methylbenzolt;agt;pyrene With iodine; silver perchlorate in benzene
Radical cation*AgI formation;
2: anhydrous tetramethylammonium acetate in water; acetonitrile
Substitution;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
in acetonitrile
0.25 h;
参考文献
Cremonesi, Paolo; Stack, Douglas E.; Rogan, Eleanor G.; Cavalieri, Ercole L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7683 - 7687