sodium hydroxide; bromine

1: tert-butyl-d9 chloride With magnesium in diethyl ether 2 h; Heating; 2: carbon dioxide in diethyl ether T=20°C; 0.5 h; 3: With sulfuric acid in diethyl ether Further stages. Title compound not separated from byproducts.;

magnesium in tetrahydrofuran

暂无反应条件数据

1: LiAlD4 2: pyridine 3: LiD, LiAlD4 / tetrahydrofuran View Scheme