(2-甲基烯丙基)三苯基氯化膦合成路线 (共 5 条)
反应条件
n-butyllithium in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Mandai, Tadakatsu; Osaka, Kazuhito; Kawagishi, Makoto; Kawada, Mikio; Otera, Junzo
Synthetic Communications, 1984 , vol. 14, # 9 p. 797 - 804
参考文献
Wolinsky,J. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2775 - 2779
反应条件
N-benzyl-trimethylammonium hydroxide
1.) reflux, 24 h, 2.) acetonitrile, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Kampmeier, J. A.; Harris, S. H.; Rodehorst, R. M.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1478 - 1485
反应条件
(i) aq. NaOH, (ii) /BRN= 4170768/, DMF; Multistep reaction;
参考文献
Narasimhan,N.S. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14, p. 329 - 331
反应条件
(i) nBuLi, heptane, Et2O, (ii) /BRN= 1700013/; Multistep reaction;
参考文献
Sorensen,T.S.
Journal of the American Chemical Society, 1965 , vol. 87, p. 5075 - 5084