苄基 alpha-D-吡喃葡萄糖苷合成路线 （共 31 条）
反应条件
1: 1.) HBr, AcOH, 2.) Ag2CO3, 4A MS / 1.) 0 deg C, 2 h, 2.) CH2Cl2, room temperature, 24 h 2: MeONa / methanol / 6 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 1 p. 144 - 152
反应条件
toluene-4-sulfonic acid T=60 - 70°C; 4 h;
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 255 - 259
反应条件
gold(III) chloride in acetonitrile 2 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 21 p. 8417 - 8420
反应条件
Prunus domestica prune seed meal T=50°C; pH=6; 42 h; aq. phosphate bufferIonic liquidEnzymatic reaction;
参考文献
Yang, Rong-Ling; Li, Ning; Zong, Min-Hua
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 74, # 1-2 p. 24 - 28
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 2: sodium methylate; methanol View Scheme
反应条件
1.1: 12.4 g / CSA / CHCl3 / 1 h / Heating 2.1: NaH / dimethylformamide / 0.5 h / 20 °C 2.2: 16.8 g / Bu4NI / dimethylformamide View Scheme
参考文献
Clausen, Mads H.; Jorgensen, Malene R.; Thorsen, Jesper; Madsen, Robert
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 5 p. 543 - 551
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=80°C; 2.5 h; Inert atmosphere;
参考文献
Zheng, Shaojun; Laraia, Luca; O'Connor, Cornelius J.; Sorrell, David; Tan, Yaw Sing; Xu, Zhaochao; Venkitaraman, Ashok R.; Wu, Wenjun; Spring, David R.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2590 - 2593
反应条件
toluene-4-sulfonic acid 4 h; Ambient temperature;
参考文献
Hoffman, James; Theander, Olof; Lindberg, Mats; Norberg, Thomas
Carbohydrate Research, 1985 , vol. 137, p. 265 - 269
反应条件
benzaldehyde; zinc(II) chloride
参考文献
Klemer
Chemische Berichte, 1959 , vol. 92, p. 218,222
反应条件
1: β-glucosidase / pH 6.2 / |Enzymatic reaction 2: Thermoplasma acidophilum glucose dehydrogenase; NADP / |Enzymatic reaction View Scheme
参考文献
Iqbal, Amjid; Chibli, Hicham; Hamilton, Chris J.
Carbohydrate Research, 2013 , vol. 377, p. 1 - 3
