反应条件
1: Ti(Oi-Pr)4, i-PrMgCl / diethyl ether / a) -45 to -40 deg C, 1 h, b) from -40 deg C to RT, 90 min, c) RT, 2 h 2: FeCl3, pyridine / dimethylformamide / 0.5 h / Ambient temperature 3: NaOAc / methanol / 1 h / Ambient temperature View Scheme
参考文献
Hareau, Georges P.-J.; Koiwa, Masakazu; Hikichi, Shinichi; Sato, Fumie
Journal of the American Chemical Society, 1999 , vol. 121, # 15 p. 3640 - 3650
