反应条件
1: methyl 3-methyl-4-iodobenzoate With isopropylmagnesium chloride in tetrahydrofuran
T=-20°C; 2 h;
2: 2,7-difluoro-3,6-bis(2-methoxyethoxymethoxy)xanthen-9-one in tetrahydrofuran
T=-20 - 22°C; 16 h;
3: With trifluoroacetic acid in dichloromethane
T=22°C; 2 h;
参考文献
Mottram, Laurie F.; Boonyarattanakalin, Siwarutt; Kovel, Rebecca E.; Peterson, Blake R.
Organic Letters, 2006 , vol. 8, # 4 p. 581 - 584