[(1S,2S,5R)-2-异丙基-5-甲基环己基](二苯基)氧膦合成路线 （共 5 条）
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in tetrahydrofuran T=65°C; 10 h;
参考文献
Yamashita, Mitsuji; Soeda, Yukio; Suzuki, Nobuyoshi; Yamada, Manabu; Tsunekawa, Kenji; et al.
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1871 - 1872
Title/Abstract Full Text Show Details
Yamashita, Mitsuji; Suzuki, Nobuyoshi; Yamada, Manabu; Soeda, Yukio; Yamashita, Hiroaki; et al.
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 219 - 222
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in tetrahydrofuran T=65°C; 5.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamashita, Mitsuji; Suzuki, Nobuyoshi; Yamada, Manabu; Soeda, Yukio; Yamashita, Hiroaki; et al.
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 219 - 222
反应条件
1: triphenylphosphine With lithium in tetrahydrofuran T=20°C; 24 h; 2: [1S-(1α,2β,4β)]-2-chloro-4-methyl-1-(methylethyl)cyclohexane in tetrahydrofuran 54 h; Heating;
参考文献
Beaumont; Kiely; Rooney
Journal of Fluorine Chemistry, 2001 , vol. 108, # 1 p. 47 - 50
反应条件
1: 71 percent / hydrobromic acid, conc. sulfuric acid / 5 h / 105 °C 2: sodium dihydridobis(2-methoxyethanolato)aluminate (SDMA) / tetrahydrofuran / 5.5 h / 65 °C View Scheme
参考文献
Yamashita, Mitsuji; Suzuki, Nobuyoshi; Yamada, Manabu; Soeda, Yukio; Yamashita, Hiroaki; et al.
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 219 - 222
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in tetrahydrofuran T=65°C; 10 h; other menthyl derivatives; var. solvents; var. temperatures; var. time; Product distribution;
参考文献
Yamashita, Mitsuji; Suzuki, Nobuyoshi; Yamada, Manabu; Soeda, Yukio; Yamashita, Hiroaki; et al.
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 219 - 222
