3，5-二甲基-4-氨基吡啶合成路线 （共 4 条）
反应条件
phosphorus trichoride in chloroform T=80°C; 22 h; Inert atmosphere;
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
titanium in tetrahydrofuran 0.25 h; Ambient temperature; Yield given;
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
1.1: sulfuric acid; nitric acid / 6 h / 20 - 90 °C 2.1: palladium 10 on activated carbon / ethanol / 1 h / 90 °C / Inert atmosphere 2.2: 3 h / 90 °C / Inert atmosphere 3.1: phosphorus trichoride / chloroform / 22 h / 80 °C / Inert atmosphere View Scheme
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
2 h; Heating;
参考文献
Ballester, Pablo; Costa, Antoni; Deya, Pere M.; Frontera, Antonio; Gomila, Rosa M.; Oliva, Ana I.; Sanders, Jeremy K. M.; Hunter, Christopher A.
Journal of Organic Chemistry, 2005 , vol. 70, # 17 p. 6616 - 6622
