N-(3-氨基苯基)环己烷甲酰胺合成路线 (共 4 条)
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran; methanol
T=40°C; P=2625.26 Torr; 24 h;
参考文献
Mohmeyer, Nils; Schmidt, Hans-Werner
Chemistry - A European Journal, 2007 , vol. 13, # 16 p. 4499 - 4509
反应条件
1: LiCl / 1-methyl-pyrrolidin-2-one; pyridine / 2 h / 80 °C
2: H2 / palladium on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C / 2625.26 Torr
View Scheme
参考文献
Mohmeyer, Nils; Schmidt, Hans-Werner
Chemistry - A European Journal, 2007 , vol. 13, # 16 p. 4499 - 4509
反应条件
1: LiCl / 1-methyl-pyrrolidin-2-one; pyridine / 2 h / 80 °C
2: H2 / palladium on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C / 2625.26 Torr
View Scheme
参考文献
Mohmeyer, Nils; Schmidt, Hans-Werner
Chemistry - A European Journal, 2007 , vol. 13, # 16 p. 4499 - 4509
反应条件
potassium carbonate; benzene
Hydrieren des Reaktionsprodukts an Nickel in Methanol bei 100grad unter Druck;
参考文献
Du Pont de Nemours and Co.
Patent: US1985601 , 1933 ;