1,2-二氯-3,3,3-三氟丙烯合成路线 (共 23 条)
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=95°C; Continous process;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: WO2004/99109 A1, 2004 ;
Location in patent: Page 8 ;
反应条件
chlorine; carbon T=200°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
INEOS FLUOR HOLDINGS LIMITED
Patent: WO2009/125199 A2, 2009 ;
Location in patent: Page/Page column 30; 31 ;
反应条件
1: With hydrogen fluoride; Catalyst M-Chromium oxide T=350°C; P=2311.54 Torr; 0.00177778 h; 2: With FeCl3/C T=180°C; P=2311.54 Torr; 0.00244444 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2009/30244 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
1: With hydrogen fluoride; 4-methoxy-phenol; Catalyst M-Chromium oxide T=350°C; P=1794.37 Torr; 0.00177778 h; 2: With FeCl3/C T=180°C; P=1794.37 Torr; 0.00244444 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2009/30244 A1, 2009 ;
Location in patent: Page/Page column 3-4 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=78 - 91°C; P=4380.18 - 6707.41 Torr; 71 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2009/182179 A1, 2009 ;
Location in patent: Page/Page column 3-7 ;
参考文献
Henne; Whaley; Stevenson
Journal of the American Chemical Society, 1941 , vol. 63, p. 3479
反应条件
hydrogen fluoride; chlorine T=140°C; Inert atmosphere;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0104; 0105 ;
反应条件
hydrogen fluoride; chlorine T=300°C; Inert atmosphere;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0104; 0105 ;
反应条件
hydrogen fluoride; chlorine T=350°C; Inert atmosphere; Temperature;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0104; 0105 ;
反应条件
antimony(V) pentachloride; SbF3
参考文献
Whaley; Davis
Journal of the American Chemical Society, 1948 , vol. 70, p. 1027