1,1,2-三氯-3,3,3-三氟丙稀合成路线 (共 179 条)
反应条件
hydrogen fluoride; chlorine; copper-substituted α-chromium oxide (99percent chromium/1percent copper) treated with HF
T=280°C; P=760.051 Torr; 0.00138889 h; Inert atmosphereMonel.(TM). nickel alloy tube packed with Monel.(TM). turnings; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Rosenfeld, H. David; Sievert, Allen; Subramoney, Shekhar
Patent: US2010/152503 A1, 2010 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen fluoride; chlorine; cobalt(II) chromite in nitrogen
T=375°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2004/18397 A1, 2004 ;
Location in patent: Page 23; 25 ;
反应条件
hydrogen fluoride; chlorine
T=280°C; P=760.051 Torr; 0.00833333 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37743 A1, 2005 ;
Location in patent: Page/Page column 15-16; 17 ;
反应条件
hydrogen fluoride; chlorine; Cr(NO3)3; AuCl3; NH4OH; calcined; Cr/Au=98/2
T=280 - 400°C; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Sievert, Allen Capron; Rosenfeld, H. David; Subramoney, Shekhar
Patent: US2008/207964 A1, 2008 ;
Location in patent: Page/Page column 14-15 ;
反应条件
hydrogen fluoride; chlorine; Cr(NO3)3[9(H2O)]; HAuCl4; AgNO3; calcined
T=280 - 400°C; 0.00138889 h; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Sievert, Allen Capron
Patent: US2008/207962 A1, 2008 ;
Location in patent: Page/Page column 12-13 ;
反应条件
hydrogen fluoride; chlorine; Cr(NO3)3[9(H2O)]; AgNO3; calcined
T=280 - 450°C; 0.00138889 - 0.00416667 h; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Sievert, Allen Capron
Patent: US2008/207963 A1, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
unter Druck in der Kaelte;
参考文献
du Pont de Nemours and Co.
Patent: US2437993 , 1946 ;
反应条件
SbF5
T=5 - 10°C; 3 h;
参考文献
Petrov, V. A.; Belen'kii, G. G.; German, L. S.; Kurbakova, A. P.; Leites, L. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 160 - 164
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 170 - 174
参考文献
Cherstkov, V. F.; Sterlin, S. R.; German, L. S.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 12 p. 2468 - 2472
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 12 p. 2791 - 2795
反应条件
hydrogen; platinum on activated charcoal in ethanol
P=6080 Torr; 5 h; Ambient temperature;
参考文献
Tanuma, T.; Ohnishi, K.; Okamoto, H.; Miyajima, T.; Morikawa, S.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 259 - 284