1,1,2-三氯-3,3,3-三氟丙稀合成路线 (共 179 条)
反应条件
hydrogen fluoride; chlorine; Cr(NO3)3[9(H2O)]; AgNO3; calcined T=280 - 450°C; 0.00138889 - 0.00416667 h; Product distribution / selectivity;
参考文献
US2008/207963 A1, ;
Page/Page column 8-9 ;
反应条件
N,N-dimethyl acetamide; zinc(II) chloride; zinc T=140 - 150°C;
参考文献
Tajammal, Sabiha; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1990 , vol. 47, p. 45 - 57
参考文献
Yagupol'skii,L.M.; Chaika,E.A.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2161 - 2165,2243 - 2247
反应条件
hydrogen fluoride; chlorine; copper-substituted α-chromium oxide (99percent chromium/1percent copper) treated with HF T=280°C; P=760.051 Torr; 0.00138889 h; Inert atmosphereMonel.(TM). nickel alloy tube packed with Monel.(TM). turnings;
参考文献
Rao, Velliyur Nott Mallikarjuna; Rosenfeld, H. David; Sievert, Allen; Subramoney, Shekhar
Patent: US2010/152503 A1, 2010 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen fluoride; chlorine; copper-substituted α-chromium oxide (99percent chromium/1percent copper) treated with HF T=375°C; P=760.051 Torr; 0.00138889 h; Inert atmosphereMonel.(TM). nickel alloy tube packed with Monel.(TM). turnings;
参考文献
Rao, Velliyur Nott Mallikarjuna; Rosenfeld, H. David; Sievert, Allen; Subramoney, Shekhar
Patent: US2010/152503 A1, 2010 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen fluoride; chlorine; chromium cobalt oxide in nitrogen T=300 - 400°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2004/18397 A1, 2004 ;
Location in patent: Page 22; 25 ;
反应条件
hydrogen fluoride; catalyst from preparation example 1 (99percent Cr/1percent Cu) T=280 - 320°C; P=760.051 Torr; 0.00138889 h; Gas phase; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2007/19358 A2, 2007 ;
Location in patent: Page/Page column 13-15 ;
反应条件
hydrogen fluoride; chlorine; chromium cobalt oxide in nitrogen T=300 - 400°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2004/18397 A1, 2004 ;
Location in patent: Page 22; 25 ;
反应条件
hydrogen fluoride; chlorine; Catalyst M-Chromium oxide in nitrogen T=300 - 400°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2004/18397 A1, 2004 ;
Location in patent: Page 17-18; 24 ;
反应条件
hydrogen fluoride; chlorine; copper-substituted α-chromium oxide (99percent chromium/1percent copper) treated with HF T=375°C; P=760.051 Torr; 0.00138889 h; Inert atmosphereMonel.(TM). nickel alloy tube packed with Monel.(TM). turnings; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Rosenfeld, H. David; Sievert, Allen; Subramoney, Shekhar
Patent: US2010/152503 A1, 2010 ;
Location in patent: Page/Page column 12 ;