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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4314-98-1
合成路线
（共 19 条）
68941-76-4
溴(3-己烷基)镁
+
4206-75-1
氯苯基硅烷
→
反应条件
反应条件
1: 1-ethylbutylmagnesium bromide With anhydrous iron chloride; tributylphosphine; copper(I) bromide in tetrahydrofuran; diethyl ether T=-25°C; 0.166667 h; Inert atmosphere; 2: phenyl-chloro-silane in tetrahydrofuran; diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
927-77-5
丙基溴化镁
→
反应条件
4314-98-1
+
17882-13-2
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: n-propyl-magnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
931-50-0
环己基溴化镁
→
反应条件
4314-98-1
+
18036-87-8
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: cyclohexyl magnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
4852-26-0
3-戊基溴化镁
→
反应条件
1351520-92-7
+
17988-45-3
+
4314-98-1
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: 3-pentylmagnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
1631-90-9
→
反应条件
4314-98-1
反应条件
暂无反应条件数据
参考文献
Harvey et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 4555
68941-76-4
溴(3-己烷基)镁
+
872-05-9
1-癸烯
+
4206-75-1
氯苯基硅烷
→
反应条件
反应条件
1: 1-n-decene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in tetrahydrofuran T=-25°C; 0.0833333 h; Inert atmosphere; 2: 1-ethylbutylmagnesium bromide in tetrahydrofuran; diethyl ether T=-25°C; 0.166667 h; Inert atmosphere; 3: phenyl-chloro-silane in tetrahydrofuran; diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
694-53-1
苯硅烷
→
反应条件
4314-98-1
反应条件
(R,R)-[La(Biphen){CH(SiMe3)2}]2 in benzene-d6 T=60°C; 22 h; Product distribution; Further Variations:Catalyststime;
参考文献
Gribkov, Denis V.; Hampel, Frank; Hultzsch, Kai C.
European Journal of Inorganic Chemistry, 2004 , # 20 p. 4091 - 4101
111-66-0
1-辛烯
+
694-53-1
苯硅烷
→
反应条件
4314-98-1
+
18899-87-1
反应条件
C25H23N3*Br2Fe; NaBEt3H T=50°C; 24 h; regioselective reaction;
参考文献
Kamata, Kouji; Suzuki, Atsuko; Nakai, Yuta; Nakazawa, Hiroshi
Organometallics, 2012 , vol. 31, # 10 p. 3825 - 3828
592-41-6
1-己烯
+
694-53-1
苯硅烷
→
反应条件
1072-14-6
三叔丁基硅烷
+
775-12-2
二苯基硅烷
+
4314-98-1
反应条件
[Cp*(iPr3P)RuH2(]SiHMes)][CB11H6Br6] T=80°C; 1 h;
参考文献
Fasulo, Meg E.; Lipke, Mark C.; Tilley, T. Don
Chemical Science, 2013 , vol. 4, # 10 p. 3882 - 3887
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