2-(4-甲酰基苯基)乙酸乙酯合成路线 （共 7 条）
参考文献
Baker et al.
Journal of the Chemical Society, 1956 , p. 404,410
反应条件
tris-(dibenzylideneacetone)dipalladium(0); i-Pr2NPPh2; water; potassium carbonate in tetrahydrofuran
T=65°C; 8 h; Inert atmosphere;
参考文献
Peng, Zhi-Yong; Wang, Jian-Ping; Cheng, Jiang; Xie, Xiao-Min; Zhang, Zhaoguo
Tetrahedron, 2010 , vol. 66, # 42 p. 8238 - 8241
反应条件
palladium diacetate; 1,3-bis(alkyl)imidazolium chloride (LHX4); caesium carbonate in 1,4-dioxane
T=80°C; 24 h;
参考文献
Oezdemir, Ismail; Yigit, Murat; Cetinkaya, Engin; Cetinkaya, Bekir
Tetrahedron Letters, 2004 , vol. 45, # 30 p. 5823 - 5825
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; sodium carbonate in acetic acid
参考文献
Merck Patent Gesellschaft Mit Beschrankter Haftung
Patent: US6028080 A1, 2000 ;
反应条件
manganese(IV) oxide in dichloromethane
19 h;
参考文献
GLAXO GROUP LIMITED; GORE, Paul Martin; HANCOCK, Ashley, Paul; HODGSON, Simon Teanby
Patent: WO2010/94643 A1, 2010 ;
Location in patent: Page/Page column 59 ;
WO 2010/094643 A1
反应条件
Raney-alloy in formic acid
1.16667 h; Heating;
参考文献
Biagi; Livi; Scartoni; Verugi
Farmaco, Edizione Scientifica, 1988 , vol. 43, # 7-8 p. 597 - 611
反应条件
1: 80 percent / NaBH4 / methanol / Ambient temperature
2: 0.620 g / 12M HCl / 1.) ice-cool, 30 min; 2.) r.t., overnight
View Scheme
参考文献
Biagi; Livi; Scartoni; Verugi
Farmaco, Edizione Scientifica, 1988 , vol. 43, # 7-8 p. 597 - 611
