(1,1-二甲氧基乙基)苯合成路线 （共 53 条）
反应条件
lithium aluminium tetrahydride; TiI4 in tetrahydrofuran T=-5°C; 0.5 h; further reagents: TiCl3-LiAlH4, TiCl4-LiAlH4, TiCl3-Mg; various conditions: t (deg C) 66-0; time (min) 60-30;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1771 - 1774
反应条件
lithium aluminium tetrahydride; TiI4 in tetrahydrofuran T=-5°C; 0.5 h; further reagents: TiCl3-LiAlH4, TiCl4-LiAlH4, TiCl3-Mg; various conditions: t (deg C) 66-0; time (min) 60-30;
参考文献
Garcia, Mariano; Campo, Carmen del; Llama, Emilio F.; Sinisterra, Jose V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 13 p. 1771 - 1774
反应条件
toluene-4-sulfonic acid T=80°C;
参考文献
Suzuki, Hitomi; Yonezawa, Shuji; Mori, Tadashi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1535 - 1544
反应条件
lithium in tetrahydrofuran T=20°C; 24 h;
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5532 - 5535
反应条件
1: pyridinium p-toluenesulfonate / benzene / 0.5 h / Heating 2: Br2AlH / diethyl ether / 1.) -78 deg C, 1 h; 2.) 0 deg C, 0.5 h 3: 1.) oxalyl chloride/DMSO; 2.) Et3N / CH2Cl2 / 1.) -78 deg C, 17 min; 2.) a.) -78 deg C, 5 min; b.) RT, 30 min 4: K2CO3 / methanol / 12 h / Ambient temperature View Scheme
参考文献
Mori, Atsunori; Fujiwara, Junya; Maruoka, Keiji; Yamamoto, Hisashi
Tetrahedron Letters, 1983 , vol. 24, # 42 p. 4581 - 4584
反应条件
in toluene T=200°C; 16 h; Inert atmosphere;
参考文献
Lee, Jennifer J.; Kraus, George A.
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2366 - 2368
反应条件
1: 63 percent / p-toluenesulfonic acid / benzene / Heating 2: 60 percent / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Narasaka, Koichi; Iwasawa, Nobuharu; Inoue, Masayuki; Yamada, Tohru; Nakashima, Masako; Sugimori, Jun
Journal of the American Chemical Society, 1989 , vol. 111, # 14 p. 5340 - 5345
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Minamikawa, Hiroyuki; Hayakawa, Satoshi; Yamada, Tohru; Iwasawa, Nobuharu; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 12 p. 4379 - 4384
反应条件
hafnium tetrachloride in acetonitrile T=20°C; Strecker Aminoacid Synthesis; 0.5 h; Inert atmosphere;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 690 - 693
反应条件
1: fired clay / 150 °C 2: sodium acetate; diluted alcohol View Scheme
参考文献
Sigmund; Uchann
Monatshefte fuer Chemie, 1929 , vol. 51, p. 250
