4,6-二氯-5-硝基嘧啶合成路线 （共 40 条）
反应条件
N,N-dimethyl-aniline; trichlorophosphate 2 h; Heating;
参考文献
Latli, Bachir; Jones, Paul-James; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Journal of Labelled Compounds and Radiopharmaceuticals, 2008 , vol. 51, # 1 p. 54 - 58
反应条件
N,N-dimethyl-aniline; trichlorophosphate
参考文献
Yamazaki, Takahisa; Komatsu, Kazunori; Umemiya, Hiroki; Hashimoto, Yuichi; Shudo, Koichi; Kagechika, Hiroyuki
Tetrahedron Letters, 1997 , vol. 38, # 48 p. 8363 - 8366
反应条件
N,N-dimethyl-aniline; trichlorophosphate
参考文献
ICI
Patent: US2557721 , 1948 ;
Full Text Show Details
Boon et al.
Journal of the Chemical Society, 1951 , p. 96,99
参考文献
Hull
Journal of the Chemical Society, 1959 , p. 481,483
参考文献
Baraldi, Pier Giovanni; Broceta, Asier Unciti; Infantas, Maria Jose Pineda De Las; Mochun, Juan Jose Diaz; Espinosa, Antonio; Romagnoli, Romeo
Tetrahedron, 2002 , vol. 58, # 38 p. 7607 - 7611
反应条件
sodium hydrogencarbonate in tetrahydrofuran T=55°C; 1 h;
参考文献
Baraldi, Pier Giovanni; Broceta, Asier Unciti; Infantas, Maria Jose Pineda De Las; Mochun, Juan Jose Diaz; Espinosa, Antonio; Romagnoli, Romeo
Tetrahedron, 2002 , vol. 58, # 38 p. 7607 - 7611
反应条件
ammonia; triethylamine in N-methyl-acetamide; dichloromethane
参考文献
Kyowa Hakko Kogyo Co., Ltd.
Patent: US6423716 B1, 2002 ;
反应条件
sodium hydrogencarbonate in tetrahydrofuran T=55°C; 1 h;
参考文献
Baraldi, Pier Giovanni; Broceta, Asier Unciti; Infantas, Maria Jose Pineda De Las; Mochun, Juan Jose Diaz; Espinosa, Antonio; Romagnoli, Romeo
Tetrahedron, 2002 , vol. 58, # 38 p. 7607 - 7611
反应条件
tin(ll) chloride in ethanol 1 h; Heating;
参考文献
Latli, Bachir; Jones, Paul-James; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Journal of Labelled Compounds and Radiopharmaceuticals, 2008 , vol. 51, # 1 p. 54 - 58
反应条件
ammonium formate; palladium on activated charcoal in methanol T=0 - 20°C; 14.5 h;
参考文献
Latli, Bachir; Jones, Paul-James; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Journal of Labelled Compounds and Radiopharmaceuticals, 2008 , vol. 51, # 1 p. 54 - 58
