N,N-二甲基-1-苯基巯基-甲胺合成路线 （共 11 条）
反应条件
(i) Mg, Et2O, (ii) /BRN= 2208235/; Multistep reaction;
参考文献
Sato,Y. et al.
Journal of Organometallic Chemistry, 1976 , vol. 113, p. 115 - 125
反应条件
1: HCl / ethanol / 1 h / Heating 2: aq. HCl / 0.5 h View Scheme
参考文献
Suzuki, Kunio; Sekiya, Minoru
Synthesis, 1981 , # 4 p. 297 - 299
反应条件
in tetrahydrofuran 60°C, 2 h;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.5.2, page 276 - 305
反应条件
in water
T=20 - 80°C; Condensation;
参考文献
Xu, Yuelian; Fletcher, Michelle; Dolbier Jr., William R.
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3460 - 3465
反应条件
hexahydrated samarium(III) chloride
T=60°C; 1.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Khairullina; Akmanov; Tyumkina; Kunakova; Ibragimov
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 2 p. 175 - 179
参考文献
Grillot; Thompson
Journal of Organic Chemistry, 1957 , vol. 22, p. 706
反应条件
sodium hydride
1.) THF, R.T., 0.5 h, 2.) overnight.; Yield given. Multistep reaction;
参考文献
Bryson, Thomas A.; Bonitz, Gordon H.; Reichel, Curtis J.; Dardis, Richard E.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 524 - 525
参考文献
Michelot,D. et al.
Bulletin de la Societe Chimique de France, 1976 , p. 1482 - 1488
反应条件
in acetonitrile
T=20°C; Methylation; 17 h;
参考文献
Xu, Yuelian; Fletcher, Michelle; Dolbier Jr., William R.
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3460 - 3465
反应条件
(i) THF, (ii) aq. NH4Cl; Multistep reaction;
参考文献
Sato,Y. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3559 - 3564
