1-(三甲基硅基)苯并三氮唑合成路线 （共 29 条）
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature 2: 95 percent / Ambient temperature 3: 78 percent / 120 °C View Scheme
参考文献
Journal of Physical Organic Chemistry, , vol. 6, # 10 p. 567 - 573
参考文献
Sheludyakov, V. D.; Sheludyakova, S. V.; Kuznetsova, M. G.; Silkina, N. N.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 4 p. 875 - 881,705 - 711
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature 2: 90 percent / Ambient temperature 3: 71 percent Spectr. / 120 °C / other alkoxycarbonylbenzotriazoles View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Pernak, Juliuzs; Fan, Wei-Qiang
Heterocycles, 1993 , vol. 36, # 6 p. 1253 - 1262
反应条件
1: 92 percent / SOCl2 / tetrahydrofuran / 0.5 h / Heating 2: 1.) Et3N, 2.) NEt4SH / 1.) C6H6, RT, 24 h, 2.) C6H6, overnight View Scheme
参考文献
Katritzky, Alan R.; Cheng, Dai; Leeming, Peter; Ghiviriga, Ion; Hartshorn, Chris M.; Steel, Peter J.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1935 - 1941
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature 2: 95 percent / Ambient temperature 3: 22 percent / 120 °C View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Pernak, Juliuzs; Fan, Wei-Qiang
Heterocycles, 1993 , vol. 36, # 6 p. 1253 - 1262
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature 2: 90 percent / Ambient temperature 3: 29 percent Spectr. / 120 °C / other alkoxycarbonylbenzotriazoles View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Pernak, Juliuzs; Fan, Wei-Qiang
Heterocycles, 1993 , vol. 36, # 6 p. 1253 - 1262
参考文献
Gasparini, J. P.; Gassend, R.; Maire, J. C.; Elguero, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 141 - 150
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature
2: 96 percent / Ambient temperature
3: 73 percent / 120 °C
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
1: SOCl2 / 0 °C
2: 35 percent
3: 67 percent Chromat. / ethanol / 3 h / Irradiation
View Scheme
参考文献
Katritzky, Alan R.; Yang, Baozhen; Abonia, Rodrigo; Insuasty, Braulio
Journal of Chemical Research - Part S, 1996 , # 12 p. 540 - 541
反应条件
1: 92 percent / SOCl2 / tetrahydrofuran / 0.5 h / Heating
2: 1.) Et3N, 2.) H2O / 1.) C6H6, RT, 24 h, 2.) C6H6, reflux
View Scheme
参考文献
Katritzky, Alan R.; Cheng, Dai; Leeming, Peter; Ghiviriga, Ion; Hartshorn, Chris M.; Steel, Peter J.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1935 - 1941
