H2SO4 in water shaking starting material 2 days in closed vessel, concentrating and treating with 3 n H2SO4, acidic liquid is partially concentrated in the cold;;
参考文献
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3598 - 3603
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Gmelin Handbook: P: MVol.C, 273, page 626 - 629
ammonolysis at 22°C (157 Torr), finally condensation to -70°C (30 min) and warming to 20°C;
参考文献
Harris, G. S.
Journal of the Chemical Society, 1958 , p. 512 - 519
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Gmelin Handbook: F: PerFHalOrg.3, 1.15, page 163 - 176
in neat (no solvent) reaction in pyrex-tube at 20°C;;
参考文献
Bennet, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1953 , p. 1565 - 1571
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Gmelin Handbook: P: MVol.C, 271, page 622 - 624
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反应条件
alkali; H2O alkaline hydrolysis;
参考文献
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3896 - 3904
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Gmelin Handbook: F: PerFHalOrg.3, 1.15, page 163 - 176
Gmelin Handbook: F: PerFHalOrg.3, 1.15, page 163 - 176
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Haszeldine, R. N.; West, B. O.
Journal of the Chemical Society, 1957 , p. 3880 - 3884
