4-(三氟甲基磺酰基)硝基苯合成路线 (共 16 条)
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Jagupolssky; Marenez
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 887
J. Gen. Chem. USSR (Engl. Transl.), 1954 , vol. 24, p. 885,886
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
参考文献
Polenov,E.A. et al.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 6 p. 1125 - 1126,1134
反应条件
1: SnCl2; aqueous HCl View Scheme
参考文献
Jagupolssky; Marenez
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 887
J. Gen. Chem. USSR (Engl. Transl.), 1954 , vol. 24, p. 885,886
反应条件
1: SnCl2; aqueous HCl 2: bromine; acetic acid View Scheme
参考文献
Jagupolssky; Marenez
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 887
J. Gen. Chem. USSR (Engl. Transl.), 1954 , vol. 24, p. 885,886
反应条件
chromium(VI) oxide
T=100°C;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
copper(I) oxide in N,N-dimethyl-formamide
T=50°C; 18 h; Inert atmosphere;
参考文献
Cullen, Steven C.; Shekhar, Shashank; Nere, Nandkishor K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12194 - 12201
反应条件
copper(I) oxide in N,N-dimethyl-formamide
T=50°C; 18 h; Inert atmosphere;
参考文献
Cullen, Steven C.; Shekhar, Shashank; Nere, Nandkishor K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12194 - 12201
反应条件
1: With nitrogen(IV) oxide; ozone in dichloromethane
T=-10°C; Kyodai-nitration; 3 h;
2: With chromium(VI) oxide; sulfuric acid
T=100°C; 8 h;
参考文献
Nose, Masatoshi; Suzuki, Hitomi
Synthesis, 2002 , # 8 p. 1065 - 1071
反应条件
1: 81 percent / sodium carbonate / tetrahydrofuran / 3 h / Ambient temperature
2: 75 - 100 °C
View Scheme
参考文献
Sekiya, Akira; Umemoto, Teruo
Chemistry Letters, 1982 , p. 1519 - 1520
反应条件
1: 54 percent / dimethylformamide
2: 64 percent / CrO3 / 100 °C
View Scheme
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300