4-(三氟甲基磺酰基)硝基苯合成路线 (共 16 条)
参考文献
Sekiya, Akira; Umemoto, Teruo
Chemistry Letters, 1982 , p. 1519 - 1520
反应条件
1: HF / 100 - 150 °C
2: CrO3; glacial acetic acid / 50 - 100 °C
View Scheme
参考文献
I. G. Farbenind.
Patent: DE682971 , 1936 ;
DRP/DRBP Org.Chem.
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Gen. Aniline Works
Patent: US2108606 , 1937 ;
反应条件
potassium carbonate; polymer-supported Pd catalyst FC 1032 in ethanol
T=110°C; Suzuki coupling; 0.25 h; microwave irradiation;
参考文献
Wang, Ying; Sauer, Daryl R.
Organic Letters, 2004 , vol. 6, # 16 p. 2793 - 2796
反应条件
potassium fluoride; tetra-phenylphosphonium bromide in dimethyl sulfoxide
T=130°C; 0.25 h;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 1 h;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 1 h;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300