5-异丙基-2-甲基-2-环己烯-1-酮合成路线 （共 38 条）
反应条件
1: 1) TMSCl, HMPA, 2) KF / 1) CuBr-SMe2 / 1) THF, -78 deg C, 2) MeOH
2: 74 percent / CuCl2 / dimethylformamide
View Scheme
参考文献
Asaoka, Morio; Aida, Toshiaki; Sonoda, Syuzo; Takei, Hisashi
Tetrahedron Letters, 1989 , vol. 30, # 50 p. 7075 - 7078
反应条件
hydrogen; Rh as electrode
electrochemical reaction;
参考文献
Deronzier, Alain
Journal de Chimie Physique et de Physico-Chimie Biologique, 1989 , vol. 86, # 1 p. 31 - 44
反应条件
hydrogen; nickel dichloride; zinc in 2-methoxy-ethanol; water
T=40°C; 6 h;
参考文献
Petrier, Christian; Luche, Jean-Louis
Tetrahedron Letters, 1987 , vol. 28, # 21 p. 2351 - 2352
反应条件
2: 70 percent / NaH / toluene; ethanol / 12.5 h / 110 - 130 °C
View Scheme
参考文献
Paquette, Leo A.; Doehner, Robert F.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5105 - 5113
反应条件
1: 70 percent / NaH / toluene; ethanol / 12.5 h / 110 - 130 °C
View Scheme
参考文献
Paquette, Leo A.; Doehner, Robert F.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5105 - 5113
参考文献
Kergomard
Annales de Chimie (Cachan, France), 1953 , vol. <12> 8, p. 153,193
反应条件
1: PhIO, TMSN3 / CH2Cl2 / -15 °C
2: tetra-n-butylammonium fluoride (TBAF) / tetrahydrofuran / 0 °C
View Scheme
参考文献
Magnus, Philip; Evans, Andrew; Lacour, Jerome
Tetrahedron Letters, 1992 , vol. 33, # 21 p. 2933 - 2936
反应条件
copper
T=280°C; dl-carvotanacetone;
参考文献
Treibs; Schmidt
Chemische Berichte, 1927 , vol. 60, p. 2339
参考文献
Eastman,R.H.; Winn,A.V.
Journal of the American Chemical Society, 1960 , vol. 82, p. 5908 - 5914
反应条件
dihydrogen peroxide in acetonitrile
Irradiation; Yields of byproduct given;
参考文献
Sonawane, H. R.; Nanjundiah, B. S.; Kelkar, R. G.
Tetrahedron, 1986 , vol. 42, # 24 p. 6673 - 6682
