(S)-(+)-1-(2-萘基)-1,2-乙二醇合成路线 (共 7 条)
反应条件
water; oxygen; palladium diacetate; sodium carbonate T=100°C; P=6080.41 Torr; 24 h; Autoclave;
参考文献
Wang, Azhong; Jiang, Huanfeng
Journal of Organic Chemistry, 2010 , vol. 75, # 7 p. 2321 - 2326
反应条件
oxygen; bismuth mandelate in dimethyl sulfoxide T=80°C; P=760 Torr; 2.3 h;
参考文献
Boisselier, Veronique Le; Dunach, Elisabet; Postel, Michele
Journal of Organometallic Chemistry, 1994 , vol. 482, # 1-2 p. 119 - 124
反应条件
sodium tetrahydroborate
参考文献
Howe; Moore; Rao
Journal of Medicinal Chemistry, 1973 , vol. 16, # 9 p. 1020 - 1023
反应条件
sodium carbonate; (S)-4,4-Br2-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]stannepin in tetrahydrofuran; water T=-10°C; 17 h; Title compound not separated from byproducts.;
参考文献
Iwasaki, Fumiaki; Maki, Toshihide; Nakashima, Waka; Onomura, Osamu; Matsumura, Yoshihiro
Organic Letters, 1999 , vol. 1, # 7 p. 969 - 972
反应条件
(3R,4S)-4-(3,5-dinitrobenzamido)-1,2,3,4-tetrahydrophenanthren-3-yl covalently linked to 3-propyl silica surface in hexane; acetic acid; isopropyl alcohol T=25°C; pH=3.6; Resolution of racemate;
参考文献
Aneja, Ritu; Luthra, Pratibha Mehta; Ahuja, Satinder
Chirality, 2010 , vol. 22, # 5 p. 479 - 485
反应条件
oxygen; palladium diacetate; toluene-4-sulfonic acid in water T=100°C; P=6080.41 Torr; 24 h;
参考文献
Wang, Azhong; Jiang, Huanfeng
Journal of Organic Chemistry, 2010 , vol. 75, # 7 p. 2321 - 2326
反应条件
tert.-butylhydroperoxide; potassium tert-butylate in water T=80°C; 8 h;
参考文献
Shaikh, Tanveer Mahammadali; Hong, Fung-E
Tetrahedron, 2013 , vol. 69, # 42 p. 8929 - 8935