3'-硝基-4'-苄氧基-2-溴苯乙酮合成路线 （共 16 条）
反应条件
boron trifluoride-tetrahydrofuran complex; (-)-(1R,2S)-1-amino-2-hydroxy-1,2,3,4-tetrahydronaphthalene in tetrahydrofuran T=0°C; 2 h; other reag., other temp.; Product distribution;
参考文献
Wilkinson, H. Scott; Tanoury, Gerald J.; Wald, Stephen A.; Senanayake, Chris H.
Organic Process Research and Development, 2002 , vol. 6, # 2 p. 146 - 148
反应条件
oxazaborolidine from cis (1R,2S)-aminoindanol and trimethylboroxine; borane in tetrahydrofuran T=-15°C;
参考文献
Hett, Robert; Fang, Qun Kevin; Gao, Yun; Hong, Yaping; Butler, Hal T.; Nie, Xiaoyi; Wald, Stephen A.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1125 - 1128
反应条件
borane in tetrahydrofuran
参考文献
Asahi Kasei Kogyo Kabushiki Kaisha
Patent: US6037362 A1, 2000 ;
反应条件
sodium formate; Triton X-100; (R,R)-TsDPEN; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in water T=28°C; 6 h; Title compound not separated from byproducts;
参考文献
Wang, Fei; Liu, Hui; Cun, Linfeng; Zhu, Jin; Deng, Jingen; Jiang, Yaozhong
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9424 - 9429
反应条件
boron trifluoride-tetrahydrofuran complex; (-)-(1R,2S)-1-amino-2-hydroxy-1,2,3,4-tetrahydronaphthalene in tetrahydrofuran T=0°C; 2 h; other reag., other temp.; Product distribution;
参考文献
Wilkinson, H. Scott; Tanoury, Gerald J.; Wald, Stephen A.; Senanayake, Chris H.
Organic Process Research and Development, 2002 , vol. 6, # 2 p. 146 - 148
反应条件
1: NaBH4 / methanol / 3 h / 20 °C
2: HOAc / methanol
3: 10.6 g / triphenylphosphine; imidazole; iodine / toluene / 3 h / Heating
View Scheme
参考文献
Mereyala, Hari Babu; Sambaru, Kalyani
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 167 - 169
