2,2,2-三氟乙基对甲苯磺酸酯合成路线 （共 41 条）
反应条件
1: 2-methoxy-ethanol With sodium hydroxide in dimethyl sulfoxide 2: 2,2,2-trifluoro-ethanol 4-methylbenzenesulfonate in dimethyl sulfoxide T=20°C; 2 h; Product distribution / selectivity;
参考文献
Nanno, Tetsuo; Deguchi, Masaki
Patent: US2008/306308 A1, 2008 ;
Location in patent: Page/Page column 7-8 ;
反应条件
sodium hydride in dimethyl sulfoxide T=20°C; 2 h; Product distribution / selectivity;
参考文献
Nanno, Tetsuo; Deguchi, Masaki
Patent: US2008/306308 A1, 2008 ;
Location in patent: Page/Page column 8-9 ;
参考文献
Lowther, Nicholas; Crook, Polly; Hall, C. Dennis
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 195 - 204
反应条件
lithium aluminium tetrahydride
参考文献
Jackson, Richard A; Townson, Michael
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1452 - 1456
反应条件
in N,N-dimethyl-formamide T=70 - 80°C; 12 h;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 56, # 23 p. 11376 - 11391
反应条件
sodium iodide; diethylene glycol
参考文献
Tiers et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 5978
反应条件
potassium fluoride; diethylene glycol T=210 - 240°C; P=500 Torr;
参考文献
Aigbirhio, Franklin I.; Pike, Victor W.; Waters, Stephen L.; Tanner, Richard J. N.
Journal of Fluorine Chemistry, 1995 , vol. 70, # 2 p. 279 - 288
反应条件
sodium hydroxide in water; N,N-dimethyl-formamide
参考文献
Bunyagidj, Chaiyun; Piotrowska, Hanna; Aldridge, Mary H.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3335 - 3336
反应条件
sodium hydroxide in methanol; dichloromethane T=20°C; 16 h;
参考文献
Miller, Stephen C.
Journal of Organic Chemistry, 2010 , vol. 75, # 13 p. 4632 - 4635
反应条件
potassium carbonate in ethanol; N,N-dimethyl-formamide
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: EP748800 A3, 1996 ;
EP 0748800 A2
