1-乙氧基-2,2,2-三氟乙醇合成路线 (共 58 条)
反应条件
potassium carbonate
T=60°C; Substitution; 12 h;
参考文献
Gong, Yuefa; Kato, Katsuya; Kimoto, Hiroshi
Synlett, 1999 , # 9 p. 1403 - 1404
反应条件
potassium carbonate
T=120°C; Substitution; 6 h;
参考文献
Gong, Yuefa; Kato, Katsuya; Kimoto, Hiroshi
Synlett, 1999 , # 9 p. 1403 - 1404
反应条件
zinc(II) chloride
T=120°C; Substitution; 24 h;
参考文献
Gong, Yuefa; Kato, Katsuya; Kimoto, Hiroshi
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 1 p. 249 - 250
参考文献
Gong; Kato; Kimoto
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 2 p. 377 - 383
反应条件
indium in water
15 h; Ambient temperature;
参考文献
Loh, Teck-Peng; Li, Xu-Ran
Tetrahedron, 1999 , vol. 55, # 17 p. 5611 - 5622
反应条件
zinc(II) iodide in 1,4-dioxane
参考文献
Kubota, Toshio; Iijima, Masahiro; Tanaka, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1351 - 1354
反应条件
n-butyllithium; 1,8-diiodo-naphthalene; di-n-butyldichlorostannane
2.) PhMe, r.t., 70 h; Yield given. Multistep reaction;
参考文献
Asao; Liu; Maruoka
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 22 p. 2507 - 2509
反应条件
5A molecular sieve; triethylamine in dichloromethane
T=20°C; 336 h;
参考文献
Titanyuk; Vorob'eva; Osipov; Beletskaya
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 5 p. 619 - 623
反应条件
5A molecular sieve in 1,4-dioxane
Substitution; 336 h;
参考文献
Ingrassia, Laurent; Mulliez, Michel
Synthesis, 1999 , # 10 p. 1731 - 1738
反应条件
5A molecular sieve in dichloromethane
T=20°C;
参考文献
Gong, Yuefa; Kato, Katsuya
Journal of Fluorine Chemistry, 2001 , vol. 111, # 1 p. 77 - 80