1,2-双(三氟甲基)苯合成路线 (共 54 条)
参考文献
Hasek,W.R. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 543 - 551
反应条件
sulfur(IV) fluoride T=120°C; 6 h;
参考文献
Hasek,W.R. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 543 - 551
反应条件
lithium aluminium tetrahydride; titanium tetrachloride; triethylamine in tetrahydrofuran 26 h; Ambient temperature;
参考文献
Wong
Synthesis, 1984 , vol. NO. 9, p. 787 - 790
反应条件
1,1,1,4,4,4-hexafluoro-2-butyne T=65°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
2,2-dimethyl-1-oxa-2-silacyclohexa-3,5-diene; 1,1,1,4,4,4-hexafluoro-2-butyne T=62°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
triethylsilane T=60 - 70°C; 10 h; Yield given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
dimethoxy dimethyl silane T=65°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
triethylsilane; 1,1,3,3-tetramethyl-2-oxa-1,3-disilacyclopentane T=60 - 70°C; 10 h; Yield given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
T=340°C; P=98800 Torr; 60 h;
参考文献
Chambers, Richard D.; Edwards, Andrew R.
Tetrahedron, 1998 , vol. 54, # 19 p. 4949 - 4964
反应条件
1,1,1,4,4,4-hexafluoro-2-butyne T=65°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269