1,2-双(三氟甲基)苯合成路线 （共 54 条）
反应条件
in benzene T=400°C; Product distribution;
参考文献
Maier, Guenther; Mihm, Gerhard; Reisenauer, Hans Peter
Chemische Berichte, 1984 , vol. 117, # 7 p. 2351 - 2368
反应条件
in pentane 65 h; Ambient temperatureIrradiationvar. temp.; Product distribution;
参考文献
Kobayashi, Yoshiro; Ando, Akiri; Kawada, Kosuke; Kumadaki, Itsumaro
Journal of the Chemical Society, Chemical Communications, 1981 , # 24 p. 1289 - 1291
反应条件
T=168°C; 48 h; Product distribution;
参考文献
Naumann, Dieter; Kischkewitz, Jurgen
Journal of Fluorine Chemistry, 1990 , vol. 47, # 2 p. 283 - 299
反应条件
T=168°C; 192 h; Product distribution;
参考文献
Naumann, Dieter; Kischkewitz, Jurgen
Journal of Fluorine Chemistry, 1990 , vol. 47, # 2 p. 283 - 299
反应条件
72 h; IrradiationThe yields, the kind of products depend on the time of the irrad. and/or the temp., and the mol. ratio. Other trifluorometh. agents investigated; Product distribution;
参考文献
Naumann,D.; Wilkes,B.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 73
反应条件
sulfuric acid; nitric acid
参考文献
Lee, Ill-Young; Gruber, Todd D.; Samuels, Amanda; Yun, Minhan; Nam, Bora; Kang, Minseo; Crowley, Kathryn; Winterroth, Benjamin; Boshoff, Helena I.; Barry III, Clifton E.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 1 p. 114 - 126
反应条件
Ni(PCy3)2Cl2; lithium triethylborohydride; nickel dichloride in tetrahydrofuran T=20°C; Inert atmosphereReflux;
参考文献
Zhao, Wenwen; Wu, Jingjing; Cao, Song
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 574 - 578
反应条件
trifluorormethanesulfonic acid Friedel-Crafts type reaction; 4 h; Inert atmosphere;
参考文献
Kethe, Anila; Tracy, Adam F.; Klumpp, Douglas A.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 12 p. 4545 - 4549
反应条件
1: HNO3, H2SO4 2: H2SO4 / 150 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 4003 - 4010
反应条件
1: HNO3, H2SO4 2: H2SO4 / 195 - 205 °C View Scheme
参考文献
Fernandez-Bolanos,J. et al.
Journal of the Chemical Society, 1960 , p. 4003 - 4010
