1-甲氧基-2-脱氧-3,5-二甲苯甲酰氧基-D-呋喃糖苷合成路线 （共 14 条）
参考文献
Duca, Maria; Malnuit, Vincent; Barbault, Florent; Benhida, Rachid
Chemical Communications, 2010 , vol. 46, # 33 p. 6162 - 6164
反应条件
sodium hydride in tetrahydrofuran T=60 - 70°C; 4 h;
参考文献
Dhimitruka, Ilirian; SantaLucia Jr., John
Synlett, 2004 , # 2 p. 335 - 337
反应条件
1: 96 percent / hydrogen chloride / 2 h 2: 85 percent / pyridine / 20 °C View Scheme
参考文献
Koegler, Martin; Busson, Roger; De Jonghe, Steven; Rozenski, Jef; Van Belle, Kristien; Louat, Thierry; Munier-Lehmann, Helne; Herdewijn, Piet
Chemistry and Biodiversity, 2012 , vol. 9, # 3 p. 536 - 556
反应条件
1: Et3N; H2O / acetone / 2 h 2: 90 percent / NaH / tetrahydrofuran / 4 h / 60 - 70 °C View Scheme
参考文献
Dhimitruka, Ilirian; SantaLucia Jr., John
Synlett, 2004 , # 2 p. 335 - 337
反应条件
1: HCl / 0.42 h / 20 °C 2: pyridine / 20 °C View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
1: HCl 2: 15 percent Spectr. / CDCl3 / 1 h View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
acetyl chloride in acetic acid T=20°C;
参考文献
McKeen, Catherine M.; Brown, Lynda J.; Nicol, Jamie T.G.; Mellor, John M.; Brown, Tom
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2267 - 2275
反应条件
chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane; C4F9SO3K in acetonitrile 12 h; Heating;
参考文献
Vorbrueggen, Helmut; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1279 - 1286
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane; acetonitrile T=24°C; 3 h;
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
反应条件
1: 35 percent / HCl / acetic acid 2: 57.8 percent / (CH3)3SiOSO2CF3 / 1,2-dichloro-ethane; acetonitrile / 3 h / 24 °C View Scheme
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
