1-甲氧基-2-脱氧-3,5-二甲苯甲酰氧基-D-呋喃糖苷合成路线 (共 14 条)
反应条件
1: HCl 2: 15 percent Spectr. / CDCl3 / 1 h View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
1: m-chloroperbenzoic acid; BF3*Et2O / CH2Cl2 2: 80 percent / Et3N / CH2Cl2 / 20 °C View Scheme
参考文献
Crey, Caroline; Dumy, Pascal; Lhomme, Jean; Kotera, Mitsuharu
Synthetic Communications, 2003 , vol. 33, # 21 p. 3727 - 3732
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
45 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Revankar, Ganapathi R.; Gupta, Pranab K.; Adams, Alexander D.; Dalley, N. Kent; McKernan, Patricia A.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 11 p. 1389 - 1396
反应条件
tin(IV) chloride
1.) CH3CN, 80 deg C, 30 min; 2.) CH3CN, r.t.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Janardhanam, Selvasekaran; Nambiar, Krishnan P.
Tetrahedron Letters, 1994 , vol. 35, # 22 p. 3657 - 3660