1: With sodium hydroxide; hydrogen in water T=140 - 150°C; P=22502.3 - 30003 Torr; 1 h; 2: With sodium hydroxide in water T=260 - 280°C; P=22502.3 - 30003 Torr; 2 h; Further stages.;
参考文献
Bazurin, Alexey A.; Krasnikov, Sergey V.; Obuchova, Tatiana A.; Danilova, Angelina S.; Balakin, Konstantin V.
Tetrahedron Letters, 2004 , vol. 45, # 35 p. 6669 - 6672
sodium phosphate buffer; lipase from Candida rugosa 6.7 h; pH 7.2; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koenigsberger, Kurt; Luna, Hector; Prasad, Kapa; Repic, Oljan; Blacklock, Thomas J.
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9029 - 9032
