苯基硫代乙内酰脲-苯丙氨酸合成路线 (共 14 条)
反应条件
triethylamine in ethanol 5 h; Heating;
参考文献
Blotny
Synthesis, 1983 , vol. No. 5, p. 391 - 392
反应条件
in nitromethane T=150°C; 0.166667 h; Microwave irradiation;
参考文献
Pepino, Ana J.; Pelaez, Walter J.; Moyano, Elizabeth L.; Argueello, Gustavo A.
European Journal of Organic Chemistry, 2012 , # 18 p. 3424 - 3430
反应条件
triethylamine in dichloromethane T=20°C; 1 h;
参考文献
Jha, Sushil; Silversides, Jon D.; Boyle, Ross W.; Archibald, Stephen J.
CrystEngComm, 2010 , vol. 12, # 6 p. 1730 - 1739
反应条件
1: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / dichloromethane; acetonitrile / 18 h / 20 °C / Inert atmosphere 2: dichloromethane / 0.5 h / 20 °C / Inert atmosphere 3: N-ethyl-N,N-diisopropylamine / acetonitrile / 8 h / 35 °C / Inert atmosphere 4: diethylamine / methanol / 0.75 h / 120 °C / Microwave irradiation View Scheme
参考文献
Zhuo, Chen; Xian, Dong; Hui, Xie; Mei, Li
Heterocycles, 2011 , vol. 83, # 5 p. 1121 - 1127
反应条件
ethanol nachfolgend Eindampfen mit Salzsaeure;
参考文献
Brautlecht
Journal of Biological Chemistry, 1912 , vol. 10, p. 144
反应条件
pyridine; sodium hydroxide anschl. Cyclisierung mit wss. HCl;
参考文献
Sjoequist
Arkiv foer Kemi, 1957 , vol. 11, p. 129,130,132
反应条件
in N,N-dimethyl-formamide T=200°C; 0.0166667 h; Microwave irradiation; optical yield given as percent de;
参考文献
European Journal of Organic Chemistry, , # 18 p. 3424 - 3430
反应条件
T=200°C; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
European Journal of Organic Chemistry, , # 18 p. 3424 - 3430
反应条件
T=250°C; 0.416667 h; Microwave irradiationneat (no solvent); optical yield given as percent de;
参考文献
European Journal of Organic Chemistry, , # 18 p. 3424 - 3430
反应条件
in N,N-dimethyl-formamide T=200°C; 0.0166667 h; Microwave irradiation; optical yield given as percent de;
参考文献
European Journal of Organic Chemistry, , # 18 p. 3424 - 3430