6-(3-甲基-2-丁烯基)-5,7-二甲氧基-2H-1-苯并吡喃-2-酮合成路线 （共 12 条）
反应条件
N,N-dimethyl-aniline
T=200°C; 8 h;
参考文献
Mali, Raghao S.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 251 - 252
反应条件
1: K2CO3, Bu4NI / acetone / Heating
2: 50 percent / N,N-dimethylaniline / 8 h / 200 °C
View Scheme
参考文献
Mali, Raghao S.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 251 - 252
反应条件
N,N-dimethyl-aniline
T=200°C; 6 h;
参考文献
Mali, Raghao S.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 251 - 252
反应条件
1: benzene / 6 h / Heating
2: N,N-dimethylaniline / 6 h / 200 °C
View Scheme
参考文献
Mali, Raghao S.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 251 - 252
反应条件
1: 6 g / BF3*Et2O / dioxane / 1 h / Ambient temperature
2: 2.2 g / sodium acetate
3: 420 mg / aqueous ammonia / methanol / cold
4: 275 mg / K2CO3 / acetone
5: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
6: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
反应条件
1: 6 g / BF3*Et2O / dioxane / 1 h / Ambient temperature
2: 2.2 g / sodium acetate
3: 420 mg / aqueous ammonia / methanol / cold
4: 275 mg / K2CO3 / acetone
5: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
6: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
反应条件
1: 2.2 g / sodium acetate
2: 420 mg / aqueous ammonia / methanol / cold
3: 275 mg / K2CO3 / acetone
4: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
5: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
反应条件
1: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
2: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
反应条件
1: 275 mg / K2CO3 / acetone
2: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
3: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
反应条件
1: 420 mg / aqueous ammonia / methanol / cold
2: 275 mg / K2CO3 / acetone
3: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C
4: 120 mg / K2CO3 / acetone
View Scheme
参考文献
Sharma, Padam N.; Shoeb, Aboo; Kapil, Randhir S.; Popli, Satya P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 11 p. 938 - 939
