3-亚苄基-2,4-戊二酮合成路线 (共 46 条)
反应条件
1: O3 / CD2Cl2 / -91 °C 2: 93 percent Spectr. / CD2Cl2 / -60 °C View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
bis(acetylacetonato) palladium; triphenylphosphine T=140°C; 48 h;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
acetic anhydride in acetic acid
参考文献
Ziegler,E. et al.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1975 , vol. 30, p. 755 - 759
反应条件
in dichloromethane-d2 T=-91°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
succinic acid anhydride in acetic acid; benzene Heating;
参考文献
Ziegler,E. et al.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1975 , vol. 30, p. 755 - 759
反应条件
in dichloromethane-d2 T=-30°C; 0.416667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
(i) THF*TiCl4, Py, CCl4, (ii) /BRN= 4157967/, DMF; Multistep reaction;
参考文献
Lehnert,W.
Synthesis, 1974 , p. 667 - 669
参考文献
Knoevenagel; Werner
Justus Liebigs Annalen der Chemie, 1894 , vol. 281, p. 80
反应条件
(i) Mg, Et2O, (ii) /BRN= 1757455/; Multistep reaction;
参考文献
Nabar,D.P.; Sunthankar,S.V.
Bulletin of the Chemical Society of Japan, 1969 , vol. 42, p. 2991 - 2993