5-氯-1,2-苯异噻唑-3(2H)-酮合成路线 （共 7 条）
反应条件
potassium hydroxide in ethanol T=20°C; Cyclization; 0.5 h;
参考文献
Shimizu, Masao; Kikumoto, Hisashi; Konakahara, Takeo; Gama, Yasuo; Shibuya, Isao
Heterocycles, 1999 , vol. 51, # 12 p. 3005 - 3012
反应条件
1: SOCl2, pyridine / benzene / Heating 2: 28percent aq. NH3 View Scheme
参考文献
Miura, Yozo
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2850 - 2852
反应条件
1: 70 percent / hydroxylamine-O-sulfonic acid (HOSA); KOH / H2O / 0.5 h / ice bath 2: 75 percent / KOH / ethanol / 0.5 h / 20 °C View Scheme
参考文献
Shimizu, Masao; Kikumoto, Hisashi; Konakahara, Takeo; Gama, Yasuo; Shibuya, Isao
Heterocycles, 1999 , vol. 51, # 12 p. 3005 - 3012
参考文献
Miura, Yozo
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2850 - 2852
反应条件
tetrachloromethane; chlorine; iron(III) chloride anschliessendes Behandeln mit NH3;
参考文献
Hart et al.
Journal of the Chemical Society, 1938 , p. 2114,2117
反应条件
tetrachloromethane; chlorine; iron(III) chloride Einleiten von Ammoniak in die Reaktionsloesung;
参考文献
Hart et al.
Journal of the Chemical Society, 1938 , p. 2114,2117
反应条件
T=20°C; Einleiten von Ammoniak in die Reaktionsloesung;
参考文献
Hart et al.
Journal of the Chemical Society, 1938 , p. 2114,2117
