2,2,2-三氟苯乙酮合成路线 （共 295 条）
反应条件
in diethyl ether T=-80 - 20°C; 2 h;
参考文献
Yamazaki, Takashi; Terajima, Tsukasa; Kawasaki-Taskasuka, Tomoko
Tetrahedron, 2008 , vol. 64, # 10 p. 2419 - 2424
反应条件
aluminium trichloride in dichloromethane 4 h; Ambient temperature;
参考文献
Kashin, A. N.; Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1329 - 1334
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1569 - 1575
反应条件
diethyl ether; phenyl-magnesium bromide
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 917
反应条件
water in acetone T=20°C; 3 h;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 4.1 p. 675 - 679
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 4 p. 754 - 759
反应条件
water in acetone T=20°C; 3 h;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 4.1 p. 675 - 679
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 4 p. 754 - 759
反应条件
bis(trifluoromethyl)cadmium*glyme in pyridine; diethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Naumann, Dieter; Finke, Martina; Lange, Horst; Dukat, Wolfgang; Tyrra, Wieland
Journal of Fluorine Chemistry, 1992 , vol. 56, # 2 p. 215 - 237
反应条件
tributylphosphine; palladium diacetate in 1-methyl-pyrrolidin-2-one T=80°C; 24 h;
参考文献
Kakino; Shimizu; Yamamoto
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 2 p. 371 - 376
反应条件
BF3·2HOAc T=155 - 160°C; 5 h;
参考文献
Winter; Dodean; Smith; Anilkumar; Burton; Gard
Journal of Fluorine Chemistry, 2005 , vol. 126, # 8 p. 1202 - 1214
反应条件
glucose dehydrogenase; D-glucose; (R)-specific alcohol dehydrogenase from Candida maris IFO10003; Reduced nicotinamide-adenine dinucleotide in dimethyl sulfoxide T=50°C; pH=8.5; aq. phosphate bufferEnzymatic reaction;
参考文献
Kawano, Shigeru; Yano, Miho; Hasegawa, Junzo; Yasohara, Yoshihiko
Bioscience, Biotechnology and Biochemistry, 2011 , vol. 75, # 6 p. 1055 - 1060
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-60°C; Swarts reaction; 3 h; Inert atmosphere;
参考文献
Tanaka, Yusuke; Ishihara, Takashi; Konno, Tsutomu
Journal of Fluorine Chemistry, 2012 , vol. 137, p. 99 - 104
