1,2-二氯四甲基二硅烷合成路线 （共 115 条）
反应条件
(i) EtMgBr, (ii) /BRN= 1736173/; Multistep reaction;
参考文献
Birkofer,L.; Stilke,R.
Chemische Berichte, 1974 , vol. 107, # 12 p. 3717 - 3722
反应条件
magnesium
1.) THF, reflux, 15 min, 2.) THF, overnight; Yield given. Multistep reaction;
参考文献
Ruehl, Karen E.; Matyjaszewski, Krzysztof
Journal of Organometallic Chemistry, 1991 , vol. 410, # 1 p. 1 - 12
反应条件
triethylamine in hexanes; diethyl ether
T=20°C;
参考文献
Wang, Ziyun; Xu, Chongying; Baum, Thomas H.
Patent: US2005/80285 A1, 2005 ;
Location in patent: Page/Page column 3 ;
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine
T=145°C; 15 h;
参考文献
Rich, Jonathan D.
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5886 - 5893
反应条件
triethylamine in benzene
参考文献
Barton,T.J.; Kilgour,J.A.
Journal of the American Chemical Society, 1976 , vol. 98, # 23 p. 7231 - 7234
反应条件
1: para-bromotoluene With magnesium in tetrahydrofuran
T=0°C;
2: 1,2-dichloro-1,1,2,2-tetramethyldisilane in tetrahydrofuran
T=0 - 20°C; 18 h;
参考文献
Shaw-Taberlet, Jennifer A.; Hamon, Jean-Rene; Roisnel, Thiery; Lapinte, Claude; Flock, Michaela; Mitterfellner, Thomas; Stueger, Harald
Journal of Organometallic Chemistry, 2007 , vol. 692, # 10 p. 2046 - 2055
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 139 - 153
反应条件
(i), (ii) /BRN= 3535268/; Multistep reaction;
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1978 , vol. 149, p. 37 - 48
反应条件
magnesium in tetrahydrofuran
参考文献
Birkofer,L.; Weniger,W.
Chemische Berichte, 1973 , vol. 106, p. 3595 - 3600
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Barton,T.J.; Kilgour,J.A.
Journal of the American Chemical Society, 1976 , vol. 98, p. 7746 - 7751
