1,2-二氯四甲基二硅烷合成路线 （共 115 条）
反应条件
2-methyl-1H-imidazole; tetra-n-butyl phosphonium chloride T=265°C; P=13689.1 Torr; 3 h; Autoclave;
参考文献
MOMENTIVE PERFORMANCE MATERIALS INC.; LEWIS, Kenrick, M.; NEELY, John, D.
Patent: WO2013/101619 A1, 2013 ;
Location in patent: Paragraph 0098; 0100 ;
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=145°C; 15 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5886 - 5893
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=140°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5886 - 5893
反应条件
in 1,3,5-trimethyl-benzene T=165°C;
参考文献
Krafft, Terry E.; Rich, Jonathan D.; McDermott, Philip J.
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5430 - 5432
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
in hexane T=20°C; 1 h; var. components molar ratios; other chlorine-containing disilanes; Product distribution;
参考文献
Brevnova, T. N.; Semenov, V. V.; Razuvaev, G. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 9 p. 2010 - 2016,1729 - 1735
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=145°C; 15 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5886 - 5893
反应条件
aluminium trichloride
参考文献
Journal of Organometallic Chemistry, , vol. 547, # 1 p. 133 - 139
反应条件
n-butyllithium; lithium bromide in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Block, Eric; Dikarev, Evgeny V.; Glass, Richard S.; Jin, Jin; Li, Bo; Li, Xiaojie; Zhang, Shao-Zhong
Journal of the American Chemical Society, 2006 , vol. 128, # 46 p. 14949 - 14961
